Qi-Hai Lu, Xiao-Li Tang, Yu-Zhe Song, Xian-Wei Zuo, Gen-Liang Han, Peng-Xun Yan, Wei-Min Liu. Thermal analysis on crystal phase synthesis of iron nitride film and its magnetic properties [J]. Acta Physica Sinica, 2019, 68(11): 118101-1
- Acta Physica Sinica
- Vol. 68, Issue 11, 118101-1 (2019)
![Phase diagram of Fe-N system[24].Fe-N体系相图[24]](/Images/highlights-null.jpg)
Fig. 2. AFM spectrum of the iron nitride film obtained by sputtering.溅射得到的氮化铁薄膜的AFM图谱
Fig. 3. XRD patterns of iron nitride films before and after annealing at different temperatures for 2 hours.不同温度退火2 h前后的氮化铁薄膜的XRD图谱
Fig. 4. XRD pattern of iron nitride films with different annealing time at 430 ℃[29].
430 ℃退火不同时间的氮化铁薄膜的XRD图谱[29]
Fig. 5. TG-DSC curves of iron nitride film (dotted line is DTG, which is the first derivative of TG).氮化铁薄膜的TG-DSC曲线(虚线为DTG, 是TG的一阶导数)
Fig. 6. In-plane VSM pattern of iron nitride films.氮化铁薄膜的面内VSM图谱
Fig. 7. In-plane & out-of-plane VSM pattern of the γ' -Fe4N film
γ' -Fe4N薄膜的面内和面外VSM图谱
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Table 1. Chemical composition, main crystal phase, and crystal form of the Fe-N at key nodes of the TG-DSC curve.
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