In this comprehensive experiment course, lithium titanate was prepared by solid-phase synthesis method and used as lithium-ion batteries anode for characterization and electrochemical testing, which focused on the research and development hotspot of “lithium-ion battery”, relied on new energy major, and took practical engineering problems as the breakthrough point. The instructional design revolved around student and outcome-based education. It was combined with courses such as synthesis and preparation of new energy materials, materials analysis and testing methods. The content involved material preparation and characterization, electrode preparation and battery assembly, and performance testing and results analysis. The design and practice of this teaching experiment will help students deepen their understanding of theoretical knowledge, master the basic manufacturing process and testing methods of lithium-ion batteries, further understand the important role of the courses they have learned in the development of the new energy field, and improve their professional identity, independent thinking ability and innovation consciousness.