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    Journals >Journal of Inorganic Materials >Volume 38 >Issue 11 >Page 1345 > Article
    • Journal of Inorganic Materials
    • Vol. 38, Issue 11, 1345 (2023)
    Consolidation of Fragile Weathered Bone Relics Using Hydroxyapatite Material as Consolidant
    Yan LIU1,2,3, Yufan ZHANG1,2,3, Ximan WANG1,2,3, Ting LI1,2,3..., Wenting MA1,2,3, Fuwei YANG1,2,3,*, Liang CHEN1,2,3, Dongyue ZHAO1,2,3 and Xiaoqin YAN1,2,3|Show fewer author(s)
    Author Affiliations
  • 11. China-Central Asia “the Belt and Road” Joint Laboratory on Human and Environment Research, Northwest University, Xi’an 710127, China
  • 22. Key Laboratory of Cultural Heritage Research and Conservation, Northwest University, Xi’an 710127, China
  • 33. School of Culture Heritage, Northwest University, Xi’an 710127, China
    • show less
    DOI: 10.15541/jim20220729 Cite this Article
    Yan LIU, Yufan ZHANG, Ximan WANG, Ting LI, Wenting MA, Fuwei YANG, Liang CHEN, Dongyue ZHAO, Xiaoqin YAN. Consolidation of Fragile Weathered Bone Relics Using Hydroxyapatite Material as Consolidant[J]. Journal of Inorganic Materials, 2023, 38(11): 1345 Copy Citation Text show less
    Calcium oxide-calcium hydrogen phosphate dispersion in alcohol at concentration of 25%
    1. Calcium oxide-calcium hydrogen phosphate dispersion in alcohol at concentration of 25%
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    Consolidation mechanism of weathered bones using calcium oxide-calcium hydrogen phosphate dispersion in alcohol as consolidant
    2. Consolidation mechanism of weathered bones using calcium oxide-calcium hydrogen phosphate dispersion in alcohol as consolidant
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    Color difference of fragile bone samples after consolidation treatment
    3. Color difference of fragile bone samples after consolidation treatment
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    Effects of consolidation way and consolidant ratio on the bone weight increment
    4. Effects of consolidation way and consolidant ratio on the bone weight increment
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    Effects of consolidation way and consolidant ratio on the bone porosity
    5. Effects of consolidation way and consolidant ratio on the bone porosity
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    Effects of consolidation way and consolidant ratio on the bone density
    6. Effects of consolidation way and consolidant ratio on the bone density
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    Effects of consolidation method and consolidant ratio on surface strength of the bones
    7. Effects of consolidation method and consolidant ratio on surface strength of the bones
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    Morphology of fragile bone sample before consolidation treatment
    8. Morphology of fragile bone sample before consolidation treatment
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    Morphologies of fragile bone samples after consolidation treatments with mass ratios of calcium oxide to calcium hydrogen phosphate at 1 : 1 (a), 1 : 3 (b), 1 : 4 (c), 1 : 5 (d), 1 : 6 (e) and 1 : 7 (f), respectively
    9. Morphologies of fragile bone samples after consolidation treatments with mass ratios of calcium oxide to calcium hydrogen phosphate at 1 : 1 (a), 1 : 3 (b), 1 : 4 (c), 1 : 5 (d), 1 : 6 (e) and 1 : 7 (f), respectively
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    EDS analysis results of fragile bone samples before and after consolidation treatment
    10. EDS analysis results of fragile bone samples before and after consolidation treatment
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    Cross-sectional topographies of fragile bone samples before and after consolidation treatments
    11. Cross-sectional topographies of fragile bone samples before and after consolidation treatments
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    Cross-sectional topographies of fragile bone samples treated by different mass ratios of calcium oxide to calcium hydrogen phosphate
    12. Cross-sectional topographies of fragile bone samples treated by different mass ratios of calcium oxide to calcium hydrogen phosphate
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    XRD results of bones before (a) and after (b) consolidation treatment
    13. XRD results of bones before (a) and after (b) consolidation treatment
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    Effect of consolidant ratio on final product
    14. Effect of consolidant ratio on final product
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    Photos of archaeological bone before (a) and after (b) consolidation treatment
    15. Photos of archaeological bone before (a) and after (b) consolidation treatment
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    GroupMass ratio
    1 : 11 : 31 : 41 : 51 : 61 : 7
    Brushing123456
    Soaking789101112
    Dripping131415161718
    Table 1. Experimental groups of different mass ratios
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    ElementWeight ratio before consolidation/%Weight ratio after consolidation/%
    C05.62
    O56.9356.32
    Na9.572.56
    Mg0.911.12
    P12.0413.23
    Ca20.5521.15
    Total100.00100.00
    Table 2. EDS analysis results of frgile bone before and after consolidation treatment
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    Ratio of CaO : CaHPO4Ca(OH)2CaHPO4Ca5(PO)4OH
    1 : 1+++-++
    1 : 3--++++
    1 : 4-+++++
    1 : 5-+++++
    1 : 6-++++
    1 : 7-+++++
    Table 3. Phases of produts under different consolidant ratios
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    Abstract
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    Yan LIU, Yufan ZHANG, Ximan WANG, Ting LI, Wenting MA, Fuwei YANG, Liang CHEN, Dongyue ZHAO, Xiaoqin YAN. Consolidation of Fragile Weathered Bone Relics Using Hydroxyapatite Material as Consolidant[J]. Journal of Inorganic Materials, 2023, 38(11): 1345
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