Superhydrophobic Surface-Assisted Preparation of Microspheres and Supraparticles and Their Applications

Mengyao Pan; Huijuan Shao; Yue Fan; Jinlong Yang; Jiaxin Liu; Zhongqian Deng; Zhenda Liu; Zhidi Chen; Jun Zhang; Kangfeng Yi; Yucai Su; Dehui Wang; Xu Deng; Fei Deng

doi:10.1007/s40820-023-01284-2

[1] S.H. Nguyen, H.K. Webb, P.J. Mahon, R.J. Crawford, E.P. Ivanova, Natural insect and plant micro-/nanostructured surfaces: an excellent selection of valuable templates with superhydrophobic and self-cleaning properties. Molecules 19(9), 13614–13630 (2014).

[2] K. Koch, B. Bhushan, W. Barthlott, Diversity of structure, morphology and wetting of plant surfaces. Soft Matter 4(10), 1943–1963 (2008).

[3] W. Barthlott, M. Mail, B. Bhushan, K. Koch, Plant surfaces: structures and functions for biomimetic innovations. Nano-Micro Lett. 9, 1–40 (2017).

[4] Y.Y. Yan, N. Gao, W. Barthlott, Mimicking natural superhydrophobic surfaces and grasping the wetting process: a review on recent progress in preparing superhydrophobic surfaces. Adv. Colloid Interfac. 169(2), 80–105 (2011).

[5] H. Liu, L. Zhang, J. Huang, J. Mao, Z. Chen et al., Smart surfaces with reversibly switchable wettability: concepts, synthesis and applications. Adv. Colloid Interface 300, 102584 (2022).

[6] F. Wang, S. Li, L. Wang, Fabrication of artificial super-hydrophobic lotus-leaf-like bamboo surfaces through soft lithography. Colloid. Surface A 513, 389–395 (2017).

[7] G.D. Bixler, B. Bhushan, Fluid drag reduction and efficient self-cleaning with rice leaf and butterfly wing bioinspired surfaces. Nanoscale 5(17), 7685–7710 (2013).

[8] F. Geyer, M. D’Acunzi, A. Sharifi-Aghili, A. Saal, N. Gao et al., When and how self-cleaning of superhydrophobic surfaces works. Sci. Adv. 6(3), 9727 (2020).

[9] K.D. Amirchand, K. Kaur, V. Singh, Biochar based self-cleaning superhydrophobic surface with aqueous desphobic properties. J. Mol. Liq. 380, 121736 (2023).

[10] J.A. Howarter, J.P. Youngblood, Self-cleaning and next generation anti-fog surfaces and coatings. Macromol. Rapid Comm. 29(6), 455–466 (2008).

[11] J. Jeevahan, M. Chandrasekaran, G. Britto Joseph, R. Durairaj, G. Mageshwaran, Superhydrophobic surfaces: a review on fundamentals, applications, and challenges. J. Coat. Technol. Res. 15, 231–250 (2018).

[12] Q. Shang, Y. Zhou, Fabrication of transparent superhydrophobic porous silica coating for self-cleaning and anti-fogging. Ceram. Int. 42(7), 8706–8712 (2016).

[13] C.J. Lai, Y.J. Chen, M.X. Wu, C.C. Wu, N.T. Tang et al., Self-cleaning and anti-fogging hierarchical structure arrays inspired by termite wing. Appl. Surf. Sci. 616, 156484 (2023).

[14] I.F. Wahab, B. Abd Razak, S.W. Teck, T.T. Azmi, M. Ibrahim et al., Fundamentals of antifogging strategies, coating techniques and properties of inorganic materials; a comprehensive review. J. Mater. Res. Technol. 23, 687–741 (2023).

[15] W. Li, Y. Zhan, S. Yu, Applications of superhydrophobic coatings in anti-icing: theory, mechanisms, impact factors, challenges and perspectives. Prog. Org. Coat. 152, 106117 (2021).

[16] Y. Wang, J. Xue, Q. Wang, Q. Chen, J. Ding, Verification of icephobic/anti-icing properties of a superhydrophobic surface. ACS Appl. Mater. Interfaces 5(8), 3370–3381 (2013).

[17] L. Cao, A.K. Jones, V.K. Sikka, J. Wu, D. Gao, Anti-icing superhydrophobic coatings. Langmuir 25(21), 12444–12448 (2009).

[18] Y. Deng, F. Xu, Z. Yin, M. Xue, Y. Chen et al., Controllable fabrication of superhydrophobic alloys surface on 304 stainless steel substrate for anti-icing performance. Ceram. Int. 49, 25135–25143 (2023).

[19] L. Wang, H. Zhao, D. Zhu, L. Yuan, H. Zhang et al., A review on ultrafast laser enabled excellent superhydrophobic anti-icing performances. Appl. Sci. 13(15), 5478 (2023).

[20] L. Feng, Z. Zhang, Z. Mai, Y. Ma, B. Liu et al., A super-hydrophobic and super-oleophilic coating mesh film for the separation of oil and water. Angew. Chem. Int. Ed. 116(15), 2046–2048 (2004).

[21] B. Chen, J. Qiu, E. Sakai, N. Kanazawa, R. Liang et al., Robust and superhydrophobic surface modification by a “paint + adhesive” method: applications in self-cleaning after oil contamination and oil-water separation. ACS Appl. Mater. Interfaces 8(27), 17659–17667 (2016).

[22] N. Wang, Y. Wang, B. Shang, P. Wen, B. Peng et al., Bioinspired one-step construction of hierarchical superhydrophobic surfaces for oil/water separation. J. Colloid Interf. Sci. 531, 300–310 (2018).

[23] X. Li, X. Chen, C. Zhao, X. Luo, Y. Jiang et al., Fabrication and research of superhydrophobic paper for oil-water separation. Mater. Chem. Phys. 304, 127808 (2023).

[24] Y. Zheng, H. Bai, Z. Huang, X. Tian, F.Q. Nie et al., Directional water collection on wetted spider silk. Nature 463(7281), 640–643 (2010).

[25] Y. Zhang, T. Wang, M. Wu, W. Wei, Durable superhydrophobic surface with hierarchical microstructures for efficient water collection. Surf. Coat. Tech. 419, 127279 (2021).

[26] R.A. Pinheiro, A.A. Silva, V.J. Trava-Airoldi, E.J. Corat, Water vapor condensation and collection by super-hydrophilic and super-hydrophobic vacnts. Diam. Relat. Mater. 87, 43–49 (2018).

[27] J. Li, Y. Zhou, W. Wang, F. Du, L. Ren, A bio-inspired superhydrophobic surface for fog collection and directional water transport. J. Alloy. Compd. 819, 152968 (2020).

[28] Q. Zhang, X. Bai, Y. Li, X. Zhang, D. Tian et al., Ultrastable super-hydrophobic surface with an ordered scaly structure for decompression and guiding liquid manipulation. ACS Nano 16(10), 16843–16852 (2022).

[29] M. Jin, X. Feng, J. Xi, J. Zhai, K. Cho et al., Super-hydrophobic PDMS surface with ultra-low adhesive force. Macromol. Rapid Comm. 26(22), 1805–1809 (2005).

[30] Y. Yang, X. Li, X. Zheng, Z. Chen, Q. Zhou et al., 3D-printed biomimetic super-hydrophobic structure for microdroplet manipulation and oil/water separation. Adv. Mater. 30(9), 1704912 (2018).

[31] X. Hong, X. Gao, L. Jiang, Application of superhydrophobic surface with high adhesive force in no lost transport of superparamagnetic microdroplet. J. Am. Chem. Soc. 129(6), 1478–1479 (2007).

[32] S. Feng, J. Delannoy, A. Malod, H. Zheng, D. Quéré et al., Tip-induced flipping of droplets on janus pillars: from local reconfiguration to global transport. Sci. Adv. 6(28), 4540 (2020).

[33] Q. Sun, D. Wang, Y. Li, J. Zhang, S. Ye et al., Surface charge printing for programmed droplet transport. Nat. Mater. 18(9), 936–941 (2019).

[34] D. Guo, J. Xiao, J. Chen, Y. Liu, C. Yu et al., Superhydrophobic “aspirator”: toward dispersion and manipulation of micro/nanoliter droplets. Small 11(35), 4491–4496 (2015).

[35] T.T. Isimjan, T. Wang, S. Rohani, A novel method to prepare superhydrophobic, UV resistance and anti-corrosion steel surface. Chem. Eng. J. 210, 182–187 (2012).

[36] T. He, Y. Wang, Y. Zhang, T. Xu, T. Liu, Super-hydrophobic surface treatment as corrosion protection for aluminum in seawater. Corros. Sci. 51(8), 1757–1761 (2009).

[37] D.W. Li, H.Y. Wang, Y. Liu, D.S. Wei, Z.X. Zhao, Large-scale fabrication of durable and robust super-hydrophobic spray coatings with excellent repairable and anti-corrosion performance. Chem. Eng. J. 367, 169–179 (2019).

[38] T. Xiang, Y. Han, Z. Guo, R. Wang, S. Zheng et al., Fabrication of inherent anticorrosion superhydrophobic surfaces on metals. ACS Sustain. Chem. Eng. 6(4), 5598–5606 (2018).

[39] Z. She, Q. Li, Z. Wang, L. Li, F. Chen et al., Researching the fabrication of anticorrosion superhydrophobic surface on magnesium alloy and its mechanical stability and durability. Chem. Eng. J. 228, 415–424 (2013).

[40] M. Ran, W. Zheng, H. Wang, Fabrication of superhydrophobic surfaces for corrosion protection: a review. Mater. Sci. Tech. 35(3), 313–326 (2019).

[41] G. Xin, C. Wu, W. Liu, Y. Rong, Y. Huang, Anti-corrosion superhydrophobic surfaces of al alloy based on micro-protrusion array structure fabricated by laser direct writing. J. Alloy. Compd. 881, 160649 (2021).

[42] N. Shirtcliffe, P. Roach, Superhydrophobicity for antifouling microfluidic surfaces. Microfluidic Diagnostics: Methods and Protocols 949, 269–281 (2013).

[43] M. Wang, Y. Zi, J. Zhu, W. Huang, Z. Zhang et al., Construction of super-hydrophobic PDMS@MOF@Cu mesh for reduced drag, anti-fouling and self-cleaning towards marine vehicle applications. Chem. Eng. J. 417, 129265 (2021).

[44] A.S. Anjum, K.C. Sun, M. Ali, R. Riaz, S.H. Jeong, Fabrication of coral-reef structured nano silica for self-cleaning and super-hydrophobic textile applications. Chem. Eng. J. 401, 125859 (2020).

[45] F. Sahin, N. Celik, A. Ceylan, S. Pekdemir, M. Ruzi et al., Antifouling superhydrophobic surfaces with bactericidal and SERS activity. Chem. Eng. J. 431, 133445 (2022).

[46] L. Zhao, Q. Liu, R. Gao, J. Wang, W. Yang et al., One-step method for the fabrication of superhydrophobic surface on magnesium alloy and its corrosion protection, antifouling performance. Corros. Sci. 80, 177–183 (2014).

[47] X. He, P. Cao, F. Tian, X. Bai, C. Yuan, Autoclaving-induced in-situ grown hierarchical structures for construction of superhydrophobic surfaces: a new route to fabricate antifouling coatings. Surf. Coat. Tech. 357, 180–188 (2019).

[48] Z. Cheng, M. Du, H. Lai, N. Zhang, K. Sun, From petal effect to lotus effect: a facile solution immersion process for the fabrication of super-hydrophobic surfaces with controlled adhesion. Nanoscale 5(7), 2776–2783 (2013).

[49] M. Spaeth, W. Barthlott, Lotus-effect®: biomimetic super-hydrophobic surfaces and their application. Adv. Sci. Techn. 60, 38–46 (2009).

[50] M.M. Stanton, R.E. Ducker, J.C. MacDonald, C.R. Lambert, W.G. McGimpsey, Super-hydrophobic, highly adhesive, polydimethylsiloxane (PDMS) surfaces. J. Colloid Interf. Sci. 367(1), 502–508 (2012).

[51] W.H. Huang, C.S. Lin, Robust superhydrophobic transparent coatings fabricated by a low-temperature sol–gel process. Appl. Surf. Sci. 305, 702–709 (2014).

[52] R. Wu, G. Chao, H. Jiang, Y. Hu, A. Pan, The superhydrophobic aluminum surface prepared by different methods. Mater. Lett. 142, 176–179 (2015).

[53] L. Feng, S. Li, Y. Li, H. Li, L. Zhang et al., Super-hydrophobic surfaces: from natural to artificial. Adv. Mater. 14(24), 1857–1860 (2002).

[54] D. Wang, Q. Sun, M.J. Hokkanen, C. Zhang, F.Y. Lin et al., Design of robust superhydrophobic surfaces. Nature 582(7810), 55–59 (2020).

[55] Z. Lei, P. Zheng, L. Niu, Y. Yang, J. Shen et al., Ultralight, robustly compressible and super-hydrophobic biomass-decorated carbonaceous melamine sponge for oil/water separation with high oil retention. Appl. Surf. Sci. 489, 922–929 (2019).

[56] H. Wang, M. Liang, J. Gao, Z. He, S. Tian et al., Super-hydrophobic coating prepared by mechanical milling method. J. Coat. Technol. Res. 19, 587–595 (2022).

[57] T. Kemala, E. Budianto, B. Soegiyono, Preparation and characterization of microspheres based on blend of poly (lactic acid) and poly (ɛ-caprolactone) with poly (vinyl alcohol) as emulsifier. Arab. J. Chem. 5(1), 103–108 (2012).

[58] K. Sahil, M. Akanksha, S. Premjeet, A. Bilandi, B. Kapoor, Microsphere: a review. Int. J. Res. Pharm. Chem. 1(4), 1184–1198 (2011).

[59] M. Lengyel, N. Kállai-Szabó, V. Antal, A.J. Laki, I. Antal, Microparticles, microspheres, and microcapsules for advanced drug delivery. Sci. Pharm. 87(3), 20 (2019).

[60] S. Wintzheimer, T. Granath, M. Oppmann, T. Kister, T. Thai et al., Supraparticles: functionality from uniform structural motifs. ACS Nano 12(6), 5093–5120 (2018).

[61] H. Tan, S. Wooh, H.J. Butt, X. Zhang, D. Lohse, Porous supraparticle assembly through self-lubricating evaporating colloidal ouzo drops. Nat. Commun. 10(1), 478 (2019).

[62] I.M. Bjørge, A.M. Costa, A.S. Silva, J.P. Vidal, J.M. Nóbrega et al., Tuneable spheroidal hydrogel particles for cell and drug encapsulation. Soft Matter 14(27), 5622–5627 (2018).

[63] W. Song, A.C. Lima, J.F. Mano, Bioinspired methodology to fabricate hydrogel spheres for multi-applications using superhydrophobic substrates. Soft Matter 6(23), 5868–5871 (2010).

[64] X. Deng, M. Paven, P. Papadopoulos, M. Ye, S. Wu et al., Solvent-free synthesis of microparticles on superamphiphobic surfaces. Angew. Chem. Int. Ed. 125(43), 11496–11499 (2013).

[65] J. Song, W. Zhang, D. Wang, Y. Fan, C. Zhang et al., Polymeric microparticles generated via confinement-free fluid instability. Adv. Mater. 33(22), 2007154 (2021).

[66] M.I. Rial-Hermida, N.M. Oliveira, A. Concheiro, C. Alvarez-Lorenzo, J. Mano, Bioinspired superamphiphobic surfaces as a tool for polymer-and solvent-independent preparation of drug-loaded spherical particles. Acta Biomater. 10(10), 4314–4322 (2014).

[67] S. Wooh, H. Huesmann, M.N. Tahir, M. Paven, K. Wichmann et al., Synthesis of mesoporous supraparticles on superamphiphobic surfaces. Adv. Mater. 27(45), 7338–7343 (2015).

[68] J. Kim, H. Hwang, H.J. Butt, S. Wooh, Designing the shape of supraparticles by controlling the apparent contact angle and contact line friction of droplets. J. Colloid Interf. Sci. 588, 157–163 (2021).

[69] X. Deng, L. Mammen, H.J. Butt, D. Vollmer, Candle soot as a template for a transparent robust superamphiphobic coating. Science 335, 67–70 (2012).

[70] Y. Huang, J. Zhou, B. Su, L. Shi, J. Wang et al., Colloidal photonic crystals with narrow stopbands assembled from low-adhesive superhydrophobic substrates. J. Am. Chem. Soc. 134(41), 17053–17058 (2012).

[71] M.B. Bigdeli, P.A. Tsai, Making photonic crystals via evaporation of nanoparticle-laden droplets on superhydrophobic microstructures. Langmuir 36(17), 4835–4841 (2020).

[72] A.M. Costa, J.F. Mano, Solvent-free strategy yields size and shape-uniform capsules. J. Am. Chem. Soc. 139(3), 1057–1060 (2017).

[73] A.M. Puga, A.C. Lima, J.F. Mano, A. Concheiro, C. Alvarez-Lorenzo, Pectin-coated chitosan microgels crosslinked on superhydrophobic surfaces for 5-fluorouracil encapsulation. Carbohyd. Polym. 98(1), 331–340 (2013).

[74] A.C. Lima, W. Song, B. Blanco-Fernandez, C. Alvarez-Lorenzo, J.F. Mano, Synthesis of temperature-responsive dextran-MA/PNIPAAm particles for controlled drug delivery using superhydrophobic surfaces. Pharm. Res-Dordr. 28(6), 1294–1305 (2011).

[75] T. Takei, K. Araki, K. Terazono, Y. Ozuno, G. Hayase et al., Highly efficient encapsulation of ingredients in poly (methyl methacrylate) capsules using a superoleophobic material. Polym. Polym. Compos. 25(2), 129–134 (2017).

[76] A.M. Costa, M. Alatorre-Meda, N.M. Oliveira, J.F. Mano, Biocompatible polymeric microparticles produced by a simple biomimetic approach. Langmuir 30(16), 4535–4539 (2014).

[77] S. Kulinich, M. Farzaneh, Ice adhesion on super-hydrophobic surfaces. Appl. Surf. Sci. 255(18), 8153–8157 (2009).

[78] S. Sakai, K. Kawakami, Synthesis and characterization of both ionically and enzymatically cross-linkable alginate. Acta Biomater. 3(4), 495–501 (2007).

[79] Y. Baimark, Y. Srisuwan, Preparation of alginate microspheres by water-in-oil emulsion method for drug delivery: effect of Ca2+ post-cross-linking. Adv. Powder Technol. 25(5), 1541–1546 (2014).

[80] T. Nakaoki, H. Yamashita, Bound states of water in poly (vinyl alcohol) hydrogel prepared by repeated freezing and melting method. J. Mol. Struct. 875(1–3), 282–287 (2008).

[81] H. Adelnia, R. Ensandoost, S.S. Moonshi, J.N. Gavgani, E.I. Vasafi et al., Freeze/thawed polyvinyl alcohol hydrogels: present, past and future. Eur. Polym. J. 164, 110974 (2022).

[82] W. Fan, W. Yan, Z. Xu, H. Ni, Formation mechanism of monodisperse, low molecular weight chitosan nanoparticles by ionic gelation technique. Colloid. Surface. B 90, 21–27 (2012).

[83] J. Liang, W. Liu, G. Yang, B. Zeng, C. Fu et al., Rapid preparation of hierarchically porous ceramic microspheres based on UV-curing-assisted molding. J. Eur. Ceram. Soc. 41(16), 232–238 (2021).

[84] W. Liu, J. Liang, G. Yang, M. Huang, C. Fu et al., Novel strategy to prepare hierarchically porous ceramic microspheres via a self-assembly method on tunable superamphiphobic surfaces. ACS Appl. Mater. Interfaces 12(40), 45429–45436 (2020).

[85] R. Luo, Y. Cao, P. Shi, C.H. Chen, Near-infrared light responsive multi-compartmental hydrogel particles synthesized through droplets assembly induced by superhydrophobic surface. Small 10, 4886–4894 (2014).

[86] A.M. Costa, M. Alatorre-Meda, C. Alvarez-Lorenzo, J.F. Mano, Superhydrophobic surfaces as a tool for the fabrication of hierarchical spherical polymeric carriers. Small 11(30), 3648–3652 (2015).

[87] T. Shpigel, A. Uziel, D.Y. Lewitus, Sphrint-printing drug delivery microspheres from polymeric melts. Eur. J. Pharm. Biopharm. 127, 398–406 (2018).

[88] Y. Fan, D.H. Wang, J.L. Yang, J.N. Song, X.M. Li et al., Top-down approach for fabrication of polymer microspheres by interfacial engineering. Chin. J. Polym. Sci. 38(12), 1286–1293 (2020).

[89] P.B. O’Donnell, J.W. McGinity, Preparation of microspheres by the solvent evaporation technique. Adv. Drug Deliver. Rev. 28(1), 25–42 (1997).

[90] A.S. Utada, A. Fernandez-Nieves, J.M. Gordillo, D.A. Weitz, Absolute instability of a liquid jet in a coflowing stream. Phys. Rev. Lett. 100(1), 014502 (2008).

[91] J.D. McGraw, J. Li, D.L. Tran, A.C. Shi, K. Dalnoki-Veress, Plateau-rayleigh instability in a torus: formation and breakup of a polymer ring. Soft Matter 6(6), 1258–1262 (2010).

[92] R. Mead-Hunter, A.J. King, B.J. Mullins, Plateau rayleigh instability simulation. Langmuir 28(17), 6731–6735 (2012).

[93] S.M. Emarati, M. Mozammel, Theoretical, fundamental and experimental study of liquid-repellency and corrosion resistance of fabricated superamphiphobic surface on Al alloy 2024. Chem. Eng. J. 387, 124046 (2020).

[94] L. Jiao, Q. Xu, J. Tong, S. Liu, Y. Hu et al., Facile preparation of pliable superamphiphobic papers with high and durable liquid repellency for anti-corrosion and open surface microfluidics. Appl. Surf. Sci. 606, 154845 (2022).

[95] B. Zhang, Y. Zeng, J. Wang, Y. Sun, J. Zhang et al., Superamphiphobic aluminum alloy with low sliding angles and acid-alkali liquids repellency. Mater. Design 188, 108479 (2020).

[96] Q. Wu, A. Gao, F. Tao, P. Yang, Understanding biomolecular crystallization on amyloid-like superhydrophobic biointerface. Adv. Mater. Interfaces 5(6), 1701065 (2018).

[97] A. Gao, Q. Wu, D. Wang, Y. Ha, Z. Chen et al., A superhydrophobic surface templated by protein self-assembly and emerging application toward protein crystallization. Adv. Mater. 28(3), 579–587 (2016).

[98] F. Gentile, M.L. Coluccio, N. Coppede, F. Mecarini, G. Das et al., Superhydrophobic surfaces as smart platforms for the analysis of diluted biological solutions. ACS Appl. Mater. Interfaces 4(6), 3213–3224 (2012).

[99] L. Jiao, J. Tong, Y. Wu, Y. Hu, H. Wu et al., Self-assembly of supraparticles on a lubricated-superamphiphobic patterned surface. Appl. Surf. Sci. 576, 151684 (2022).

[100] H. Tan, S. Wooh, H.J. Butt, X. Zhang, D. Lohse, Porous supraparticle assembly through self-lubricating evaporating colloidal ouzo drops. Nat. Commun. 10(1), 1–8 (2019).

[101] L. Jiao, Y. Wu, Y. Hu, Q. Guo, H. Wu et al., Mosaic patterned surfaces toward generating hardly-volatile capsular droplet arrays for high-precision droplet-based storage and detection. Small 19(14), 2206274 (2023).

[102] T. Sekido, S. Wooh, R. Fuchs, M. Kappl, Y. Nakamura et al., Controlling the structure of supraballs by pH-responsive particle assembly. Langmuir 33(8), 1995–2002 (2017).

[103] V. Rastogi, A.A. García, M. Marquez, O.D. Velev, Anisotropic particle synthesis inside droplet templates on superhydrophobic surfaces. Macromol. Rapid Comm. 31(2), 190–195 (2010).

[104] M. Hu, H.J. Butt, K. Landfester, M.B. Bannwarth, S. Wooh et al., Shaping the assembly of superparamagnetic nanoparticles. ACS Nano 13(3), 3015–3022 (2019).

[105] W. Liu, M. Kappl, H.J. Butt, Tuning the porosity of supraparticles. ACS Nano 13(12), 13949–13956 (2019).

[106] V. Rastogi, S. Melle, O.G. Calderón, A.A. García, M. Marquez et al., Synthesis of light-diffracting assemblies from microspheres and nanoparticles in droplets on a superhydrophobic surface. Adv. Mater. 20(22), 4263–4268 (2008).

[107] S.S. Liu, C.F. Wang, X.Q. Wang, J. Zhang, Y. Tian et al., Tunable janus colloidal photonic crystal supraballs with dual photonic band gaps. J. Mater. Chem. C 2(44), 9431–9438 (2014).

[108] W. Shim, C.S. Moon, H. Kim, H.S. Kim, H. Zhang et al., Tailoring the morphology of supraparticles by primary colloids with different shapes, sizes and dispersities. Crystals 11(2), 79 (2021).

[109] L. Pauchard, Y. Couder, Invagination during the collapse of an inhomogeneous spheroidal shell. Epl-Europhys Lett. 66(5), 667 (2004).

[110] B. Yu, H. Cong, H. Yuan, X. Liu, Q. Peng et al., Preparation of doughnut-like nanocomposite colloidal crystal particles with enhanced light diffraction using drying self-assembly method. Macromol. Rapid Comm. 11(2), 161–165 (2015).

[111] R.D. Deegan, O. Bakajin, T.F. Dupont, G. Huber, S.R. Nagel et al., Capillary flow as the cause of ring stains from dried liquid drops. Nature 389(6653), 827–829 (1997).

[112] D.W. Lee, M.H. Jin, C.B. Lee, D. Oh, S.K. Ryi et al., Facile synthesis of mesoporous silica and titania supraparticles by a meniscus templating route on a superhydrophobic surface and their application to adsorbents. Nanoscale 6(7), 3483–3487 (2014).

[113] A. Accardo, F. Di Stasio, M. Burghammer, C. Riekel, R. Krahne, Nanocrystal self-assembly into hollow dome-shaped microstructures by slow solvent evaporation on superhydrophobic substrates. Part. Part. Syst. Char. 32(5), 524–528 (2015).

[114] L. Chen, J.R. Evans, Drying of colloidal droplets on superhydrophobic surfaces. J. Colloid Interf. Sci. 351(1), 283–287 (2010).

[115] M. Sperling, O.D. Velev, M. Gradzielski, Controlling the shape of evaporating droplets by ionic strength: formation of highly anisometric silica supraparticles. Angew. Chem. Int. Ed. 53(2), 586–590 (2014).

[116] M. Sperling, P. Papadopoulos, M. Gradzielski, Understanding the formation of anisometric supraparticles: a mechanistic look inside droplets drying on a superhydrophobic surface. Langmuir 32(27), 6902–6908 (2016).

[117] M. Sperling, V.J. Spiering, O.D. Velev, M. Gradzielski, Controlled formation of patchy anisometric fumed silica supraparticles in droplets on bent superhydrophobic surfaces. Part Part Syst. Char. 34(1), 1600176 (2017).

[118] Y. Hu, B. Zhao, S. Lin, X. Deng, L. Chen, Evaporation and particle deposition of bi-component colloidal droplets on a superhydrophobic surface. Int. J. Heat Mass Tran. 159, 120063 (2020).

[119] J. Zhou, J. Yang, Z. Gu, G. Zhang, Y. Wei et al., Controllable fabrication of noniridescent microshaped photonic crystal assemblies by dynamic three-phase contact line behaviors on superhydrophobic substrates. ACS Appl. Mater. Interfaces 7(40), 22644–22651 (2015).

[120] R.K. Shah, J.W. Kim, D.A. Weitz, Janus supraparticles by induced phase separation of nanoparticles in droplets. Adv. Mater. 21(19), 1949–1953 (2009).

[121] G. Yang, H. Zhong, R. Liu, Y. Li, B. Zou, In-situ aggregation of ZnSe nanoparticles into supraparticles: shape control and doping effects. Langmuir 29(6), 1970–1976 (2013).

[122] Y. Xia, T.D. Nguyen, M. Yang, B. Lee, A. Santos et al., Self-assembly of self-limiting monodisperse supraparticles from polydisperse nanoparticles. Nat. Nanotechnol. 7(7), 479–479 (2012).

[123] W. Liu, J. Midya, M. Kappl, H.J. Butt, A. Nikoubashman, Segregation in drying binary colloidal droplets. ACS Nano 13(5), 4972–4979 (2019).

[124] X.D. Meng, R. Al-Salman, J.P. Zhao, N. Borissenko, Y. Li et al., Electrodeposition of 3D ordered macroporous germanium from ionic liquids: A feasible method to make photonic crystals with a high dielectric constant. Angew. Chem. Int. Ed. 48(15), 2703–2707 (2009).

[125] X. Zhang, Y. Niu, J. Zhao, Y. Li, Self-assembly, structural order and mechanism of γ-Fe2O3@SiO2 ellipsoids induced by magnetic fields. New J. Chem. 40(11), 9520–9525 (2016).

[126] G. von Freymann, V. Kitaev, B.V. Lotsch, G.A. Ozin, Bottom-up assembly of photonic crystals. Chem. Soc. Rev. 42(7), 2528–2554 (2013).

[127] J. Hou, H. Zhang, Q. Yang, M. Li, Y. Song et al., Bio-inspired photonic-crystal microchip for fluorescent ultratrace detection. Angew. Chem. Inter. Ed. 53(23), 5791–5795 (2014).

[128] J. Hou, H. Zhang, Q. Yang, M. Li, L. Jiang et al., Hydrophilic–hydrophobic patterned molecularly imprinted photonic crystal sensors for high-sensitive colorimetric detection of tetracycline. Small 11(23), 2738–2742 (2015).

[129] R. De Angelis, I. Venditti, I. Fratoddi, F. De Matteis, P. Prosposito et al., From nanospheres to microribbons: Self-assembled eosin Y doped PMMA nanoparticles as photonic crystals. J. Colloid Interf. Sci. 414, 24–32 (2014).

[130] M. Li, X. Lai, C. Li, Y. Song, Recent advantages of colloidal photonic crystals and their applications for luminescence enhancement. Mater. Today Nano 6, 100039 (2019).

[131] M.Y. Pan, X.B. Li, C.J. Xiong, X.Y. Chen, L.B. Wang et al., Robust and flexible colloidal photonic crystal films with bending strain-independent structural colors for anticounterfeiting. Part. Part. Syst. Char. 37(4), 7 (2020)

[132] M.Y. Pan, C.Y. Wang, Y.F. Hu, X. Wang, L. Pan et al., Dual optical information-encrypted/decrypted invisible photonic patterns based on controlled wettability. Adv. Opt. Mater. 10, 2101268 (2021).

[133] C. Xiong, J. Zhao, L. Wang, H. Geng, H. Xu et al., Trace detection of homologues and isomers based on hollow mesoporous silica sphere photonic crystals. Mater. Horiz. 4(5), 862–868 (2017).

[134] X.Y. Fan, M. Xu, W.Z. Liu, A. Kuchmizhak, L. Pattelli et al., Resolving molecular size and homologues with a self-assembled metal-organic framework photonic crystal detector. ACS Mater. Lett. 5(6), 1703–1709 (2023).

[135] H. Yang, L. Pan, Y. Han, L. Ma, Y. Li et al., A visual water vapor photonic crystal sensor with PVA/SiO2 opal structure. Appl. Surf. Sci. 423, 421–425 (2017).

[136] M. Pan, L. Wang, S. Dou, J. Zhao, H. Xu et al., Recent advances in colloidal photonic crystal-based anti-counterfeiting materials. Crystals 9(8), 417 (2019).

[137] Á.G. Marín, H. Gelderblom, A. Susarrey-Arce, A. van Houselt, L. Lefferts et al., Building microscopic soccer balls with evaporating colloidal fakir drops. Proc. Natl. Acad. Sci. 109(41), 16455–16458 (2012).

[138] M. Xiao, J. Liu, Z. Chen, W. Liu, C. Zhang et al., Magnetic assembly and manipulation of janus photonic crystal supraparticles from a colloidal mixture of spheres and ellipsoids. J. Mater. Chem. C 9(35), 11788–11793 (2021).

[139] Z. Yu, C.F. Wang, L. Ling, L. Chen, S. Chen, Triphase microfluidic-directed self-assembly: anisotropic colloidal photonic crystal supraparticles and multicolor patterns made easy. Angew. Chem. Int. Ed. 10(124), 2425–2428 (2012).

[140] J. Liu, M. Xiao, C. Li, H. Li, Z. Wu et al., Rugby-ball-like photonic crystal supraparticles with non-close-packed structures and multiple magneto-optical responses. J. Mater. Chem. C 7(47), 15042–15048 (2019).

[141] S.J. Yeo, F. Tu, S.H. Kim, G.R. Yi, P.J. Yoo et al., Angle- and strain-independent coloured free-standing films incorporating non-spherical colloidal photonic crystals. Soft Matter 11(8), 1582–1588 (2015).

[142] K. Hou, J. Han, Z. Tang, Formation of supraparticles and their application in catalysis. ACS Mater. Lett. 2(1), 95–106 (2019).

[143] J. Schneider, M. Matsuoka, M. Takeuchi, J. Zhang, Y. Horiuchi et al., Understanding TiO2 photocatalysis: mechanisms and materials. Chem. Rev. 114(19), 9919–9986 (2014).

[144] S.H. Ahn, D.J. Kim, W.S. Chi, J.H. Kim, Hierarchical double-shell nanostructures of TiO2 nanosheets on SnO2 hollow spheres for high-efficiency, solid-state, dye-sensitized solar cells. Adv. Funct. Mater. 24(32), 5037–5044 (2014).

[145] C. Cheng, A. Amini, C. Zhu, Z. Xu, H. Song et al., Enhanced photocatalytic performance of TiO2-ZnO hybrid nanostructures. Sci. Rep. 4(1), 4181 (2014).

[146] M. Sperling, H.J. Kim, O.D. Velev, M. Gradzielski, Active steerable catalytic supraparticles shuttling on preprogrammed vertical trajectories. Adv. Mater. Interfaces 3(15), 1600095 (2016).

[147] H.J. Kim, M. Sperling, O.D. Velev, M. Gradzielski, Silica supraparticles with self-oscillatory vertical propulsion: mechanism & theoretical description. Part. Part. Syst. Char. 39(7), 2200021 (2022).

[148] H.E. Oguztürk, L.J. Bauer, I. Mantouvalou, B. Kanngier, O.D. Velev et al., Preparation of reinforced anisometric patchy supraparticles for self-propulsion. Part. Part. Syst. Char. 38(6), 2000328 (2021).

[149] L.H. Lim, D.G. Macdonald, G.A. Hill, Hydrolysis of starch particles using immobilized barley α-amylase. Biochem. Eng. J. 13(1), 53–62 (2003).

[150] C. Yousry, M.M. Amin, A.H. Elshafeey, O.N.E.I. Gazayerly, Ultrahigh verapamil-loaded controlled release polymeric beads using superamphiphobic substrate: d-optimal statistical design, in vitro and in vivo performance. Drug Deliv. 25(1), 1448–1460 (2018).

[151] A.C. Lima, C.R. Correia, M.B. Oliveira, J.F. Mano, Sequential ionic and thermogelation of chitosan spherical hydrogels prepared using superhydrophobic surfaces to immobilize cells and drugs. J. Bioact. Compat. Pol. 29(1), 50–65 (2014).

[152] E. Caló, V.V. Khutoryanskiy, Biomedical applications of hydrogels: a review of patents and commercial products. Eur. Polym. J. 65, 252–267 (2015).

[153] E. Ruel-Gariepy, J.C. Leroux, In situ-forming hydrogels-review of temperature-sensitive systems. Eur. J. Pharm. Biopharm. 58(2), 409–426 (2004).

[154] P.M. Reddy, P. Venkatesu, Ionic liquid modifies the lower critical solution temperature (LCST) of poly (N-isopropylacrylamide) in aqueous solution. J. Phys. Chem. B 115(16), 4752–4757 (2011).

[155] Y.K. Jhon, R.R. Bhat, C. Jeong, O.J. Rojas, I. Szleifer et al., Salt-induced depression of lower critical solution temperature in a surface-grafted neutral thermoresponsive polymer. Macromol. Rapid Comm. 27(9), 697–701 (2006).

[156] L. Hosta-Rigau, O. Shimoni, B. Städler, F. Caruso, Advanced subcompartmentalized microreactors: polymer hydrogel carriers encapsulating polymer capsules and liposomes. Small 9(21), 3573–3583 (2013).

[157] R. Chandrawati, F. Caruso, Biomimetic liposome-and polymersome-based multicompartmentalized assemblies. Langmuir 28(39), 13798–13807 (2012).

[158] A.C. Lima, C.A. Custódio, C. Alvarez-Lorenzo, J.F. Mano, Biomimetic methodology to produce polymeric multilayered particles for biotechnological and biomedical applications. Small 9(15), 2487–2492 (2013).

[159] Z. Zha, X. Yue, Q. Ren, Z. Dai, Uniform polypyrrole nanoparticles with high photothermal conversion efficiency for photothermal ablation of cancer cells. Adv. Mater. 25(5), 777–782 (2013).

[160] Y. Dong, M. Gong, D. Huang, J. Gao, Q. Zhou, Shape memory, self-healing property, and NIR photothermal effect of epoxy resin coating with polydopamine@polypyrrole nanoparticles. Prog. Org. Coat. 136, 105232 (2019).

[161] D. Yang, B. Zhou, G. Han, Y. Feng, J. Ma et al., Flexible transparent polypyrrole-decorated mxene-based film with excellent photothermal energy conversion performance. ACS Appl. Mater. Interfaces 13(7), 8909–8918 (2021).

[162] C. Schlaich, Y. Fan, P. Dey, J. Cui, Q. Wei et al., Universal, surfactant-free preparation of hydrogel beads on superamphiphobic and slippery surfaces. Adv. Mater. Interfaces 5(7), 1701536 (2018).

[163] A. Schoubben, P. Blasi, S. Giovagnoli, C. Rossi, M. Ricci, Development of a scalable procedure for fine calcium alginate particle preparation. Chem. Eng. J. 160(1), 363–369 (2010).

[164] J.W. Krumpfer, T.J. McCarthy, Dip-coating crystallization on a superhydrophobic surface: a million mounted crystals in a 1 cm2 array. J. Am. Chem. Soc. 133(15), 5764–5766 (2011).

[165] R. Nelson, M.R. Sawaya, M. Balbirnie, A.Ø. Madsen, C. Riekel et al., Structure of the cross-β spine of amyloid-like fibrils. Nature 435(7043), 773–778 (2005).

[166] C.Y. Zhang, H.F. Shen, Q.J. Wang, Y.Z. Guo, J. He et al., An investigation of the effects of self-assembled monolayers on protein crystallisation. Int. J. Mol. Sci. 14(6), 12329–12345 (2013).

[167] F. Shao, T.W. Ng, O.W. Liew, J. Fu, T. Sridhar, Evaporative preconcentration and cryopreservation of fluorescent analytes using superhydrophobic surfaces. Soft Matter 8(13), 3563–3569 (2012).

[168] L. Cai, F. Bian, L. Sun, H. Wang, Y. Zhao, Condensing-enriched magnetic photonic barcodes on superhydrophobic surface for ultrasensitive multiple detection. Lab Chip 19(10), 1783–1789 (2019).

[169] L.P. Xu, Y. Chen, G. Yang, W. Shi, B. Dai et al., Ultratrace DNA detection based on the condensing-enrichment effect of superwettable microchips. Adv. Mater. 27(43), 6878–6884 (2015).

[170] Y. Sun, X. Chen, Y. Zheng, Y. Song, H. Zhang et al., Surface-enhanced raman scattering trace-detection platform based on continuous-rolling-assisted evaporation on superhydrophobic surfaces. ACS Appl. Nano Mater. 3(5), 4767–4776 (2020).

[171] M. Fan, F. Cheng, C. Wang, Z. Gong, C. Tang et al., SERS optrode as a “fishing rod” to direct pre-concentrate analytes from superhydrophobic surfaces. Chem. Commun. 51(10), 1965–1968 (2015).

[172] Z. Wang, L. Feng, D. Xiao, N. Li, Y. Li et al., A silver nanoislands on silica spheres platform: Enriching trace amounts of analytes for ultrasensitive and reproducible sers detection. Nanoscale 9(43), 16749–16754 (2017).

[173] F. De Angelis, F. Gentile, F. Mecarini, G. Das, M. Moretti et al., Breaking the diffusion limit with super-hydrophobic delivery of molecules to plasmonic nanofocusing sers structures. Nat. Photonics 5(11), 682–687 (2011).

[174] H. Kang, Y.J. Heo, D.J. Kim, J.H. Kim, T.Y. Jeon et al., Droplet-guiding superhydrophobic arrays of plasmonic microposts for molecular concentration and detection. ACS Appl. Mater. Interfaces 9(42), 37201–37209 (2017).

[175] W. Song, D. Psaltis, K.B. Crozier, Superhydrophobic bull’s-eye for surface-enhanced raman scattering. Lab Chip 14(20), 3907–3911 (2014).

微信扫一扫：分享

微信扫一扫：分享