• Journal of Inorganic Materials
  • Vol. 39, Issue 4, 399 (2024)
Yifan XUE1, Weijie LI2,*, Zhongwei ZHANG1,*, Xu PANG1, and Yu LIU3
Author Affiliations
  • 11. Institute of Advanced Structure Technology, Beijing Institute of Technology, Beijing 100081, China
  • 22. School of Civil Engneering, Beijing Jiaotong University, Beijing 100044, China
  • 33. State Key Laboratory of Powder Metallurgy, Powder Metallurgy Research Institute, Central South University, Changsha 410083, China
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    DOI: 10.15541/jim20230512 Cite this Article
    Yifan XUE, Weijie LI, Zhongwei ZHANG, Xu PANG, Yu LIU. Process Control of PyC Interphases Microstructure and Uniformity in Carbon Fiber Cloth[J]. Journal of Inorganic Materials, 2024, 39(4): 399 Copy Citation Text show less
    Schematic diagram of mold
    1. Schematic diagram of mold
    Group 1 SEM images
    S1. Group 1 SEM images
    Group 2 SEM images
    S2. Group 2 SEM images
    TEM charaterizations of three typical samples
    2. TEM charaterizations of three typical samples
    (a) XRD patterns and (b) Raman spectra of PyC interphase on carbon fiber prepared by different fabrication processes
    3. (a) XRD patterns and (b) Raman spectra of PyC interphase on carbon fiber prepared by different fabrication processes
    Group 3 SEM images
    S3. Group 3 SEM images
    Deposition mechanism and boundary conditions for
    4. Deposition mechanism and boundary conditions for
    Group 4 SEM images
    S4. Group 4 SEM images
    Group 5 SEM images
    S5. Group 5 SEM images
    (a) Fixture layout diagram, (b) fixture main view and (c) sampling position of fiber fabric
    5. (a) Fixture layout diagram, (b) fixture main view and (c) sampling position of fiber fabric
    Group 6 SEM images
    S6. Group 6 SEM images
    Deposition rate, uniformity and typical SEM images of cross-section of PyC interphases at various temperatures
    6. Deposition rate, uniformity and typical SEM images of cross-section of PyC interphases at various temperatures
    Group 7 SEM images
    S7. Group 7 SEM images
    Deposition rate, uniformity and typical SEM images of cross-section of PyC interphases at various pC3H6
    7. Deposition rate, uniformity and typical SEM images of cross-section of PyC interphases at various pC3H6
    Group 8 SEM images
    S8. Group 8 SEM images
    Deposition rate, uniformity and typical SEM images of cross-section of PyC interphases at various residence time
    8. Deposition rate, uniformity and typical SEM images of cross-section of PyC interphases at various residence time
    Group 9 SEM images
    S9. Group 9 SEM images
    Deposition rate, uniformity and typical SEM images of cross-section of PyC interphases at various pC3H6 : pH2
    9. Deposition rate, uniformity and typical SEM images of cross-section of PyC interphases at various pC3H6 : pH2
    Relationship between interphase deposition rate, deposition uniformity and texture of PyC interphase
    10. Relationship between interphase deposition rate, deposition uniformity and texture of PyC interphase
    Group 10 SEM images
    S10. Group 10 SEM images
    Group 11 SEM images
    S11. Group 11 SEM images
    Influence factors of interphase uniformity and their relations with process parameters
    11. Influence factors of interphase uniformity and their relations with process parameters
    Group 12 SEM images
    S12. Group 12 SEM images
    Group 13 SEM images
    S13. Group 13 SEM images
    Group 14 SEM images
    S14. Group 14 SEM images
    Group 15 SEM images
    S15. Group 15 SEM images
    Group 16 SEM images
    S16. Group 16 SEM images
    Group 17 SEM images
    S17. Group 17 SEM images
    Group 18 SEM images
    S18. Group 18 SEM images
    Group 19 SEM images
    S19. Group 19 SEM images
    Group 20 SEM images
    S20. Group 20 SEM images
    GroupT/℃ pC3H6/kPa τ/s pH2/kPa
    1950530
    2950330
    3950310
    4950110
    59500.510
    6950130
    795010.50
    8900310
    990010.50
    10900130
    11900110
    1285010.50
    13850110
    14850130
    15950331.5
    16950333
    17950130.5
    18950131
    19900311.5
    20900313
    Table 1. Design parameters for experiment
    12345678910
    XRD FWHM/(°)5.5225.4955.2175.6645.8095.5795.4695.8055.8835.942
    ID/IG0.9950.9790.9910.9880.9981.0210.9910.9941.0011.050
    TextureHTMTLT
    11121314151617181920
    XRD FWHM/(°)5.9266.0565.8735.9405.5185.5975.6235.9615.7735.914
    ID/IG1.0281.0311.0371.0330.9780.9741.0110.9921.0121.003
    TextureLTHTMTLT
    Table 2. Summary of XRD FWHM and R (R=ID/IG) for Raman spectra of PyC interphases, and texture classifications
    Yifan XUE, Weijie LI, Zhongwei ZHANG, Xu PANG, Yu LIU. Process Control of PyC Interphases Microstructure and Uniformity in Carbon Fiber Cloth[J]. Journal of Inorganic Materials, 2024, 39(4): 399
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