Xin-Cun PENG, Zhi-Dong WANG, Meng-Si ZENG, Yun LIU, Ji-Jun ZOU, Zhi-Fu ZHU, Wen-Juan DENG. Improvement on Size Uniformity of SiO2 Nanospheres Applied in Si Optical Resonance Nanopillar-arrays [J]. Journal of Inorganic Materials, 2019, 34(7): 734

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- Journal of Inorganic Materials
- Vol. 34, Issue 7, 734 (2019)

1. Fabrication process of Si nanopillar-arrays by self- assembled nanosphere etching

2. Fabrication process of the monodisperse SiO2 nanospheres by two-step Stober method

3. (a) Effect of ammonia amount on particle size distribution of nanospheres; (b) Effect of TEOS amount on particle size distribution of nanospheres; (c) Fusion of the nanospheres found in the SEM image; (d) Particle size distribution of the SiO2 nanosphere seed solution under the optimized synthesis condition

4. Effect of the last-step reaction time of the two-step Stober method on uniformity of SiO2 nanospheres: (a) 1 h, (b) 2 h, (c) 3 h, (d) 4 h, (e) 5 h ; (f) Dependence of the average particle size and its distribution on reaction time; (g) SEM image of the SiO2 nanospheres with reaction time of 4 h

5. (a) SEM image of the single-layer SiO2 nanosphere on Si substrate (top view) and SEM images of the Si nanopillar-arrays from (b) top view and (c) side view

6. (a) Measured area for the light reflectance spectrum and (b) surface reflectance spectra of Si nanopillar-array samples

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